CRYSTALLOGRAPHY AND INSTRUMENTAL ANALYSIS Single channel
Chair (Coordinator) and Rapporteur: FERDINANDO BOSI
Lecturers
Objectives
Developing competences and expected learning outcomes
Educational goals:
The course gives a basic knowledge of the analytical techniques and methodology for the mineralogy, the way atoms aggregate to form minerals, of the physical properties that allow identification of minerals
Learning outcomes:
Who have taken this course should be reasonably comfortable in characterization and identification of minerals, understanding experimental data, consulting much of what appears in the mineralogical literature such as reference volumes and articles. At the end of the course, the student will be able to read and understand, at least at a basic level, a scientific paper describing a mineral. The student will be able to characterize, at least at a basic level, a mineral, to process the acquired data.
Learning outcomes
The course gives a basic knowledge of the analytical techniques and methodology for the mineralogy, the way atoms aggregate to form minerals, of the physical properties that allow identification of minerals
Who have taken this course should be reasonably comfortable in characterization and identification of minerals, understanding experimental data, consulting much of what appears in the mineralogical literature such as reference volumes and articles. At the end of the course, the student will be able to read and understand, at least at a basic level, a scientific paper describing a mineral. The student will be able to characterize, at least at a basic level, a mineral, to process the acquired data.
Prerequisites
Identification of main minerals in commonly found in igneous, sedimentary, and metamorphic rocks.
From Chemistry: atomic structure, size of atoms and ions, chemical bond, property of the elements of periodic table.
Form Mineralogy: symmetry elements, lattice space, Laue and Miller indices, point and space group, ionic radii, coordination polyhedra, Pauling rules, phase diagrams, polymorphism, compositional variation in minerals, solid solutions, optical mineralogy, X-ray diffraction, Bragg law, mineral identification, electron probe microanalysis, conversion of chemical analyses to structural formulae.
Programme
CHARACTERIZATION OF MINERALS
Course contents
The course is based on lectures (24h), laboratory (12h) and practices (24h). In detail, the course contents are as follows.
- Mineral definition. Mineral formula. Amorphous and crystalline state. Crystalline structures.
- Crystal lattice. The unit cell. The structural motif. The asymmetric unit. Point groups. Space groups. Hauy’s law of the indexes rationality.
- Crystal-chemical aspects of minerals, isomorphism, and type of structure (isotypes, homeotypes, hetreotypes).
- X-ray crystallography. Diffusion phenomenon and interaction with the crystalline matter. Diffraction. Bragg Law. Miller indices. Ewald sphere. Structure factor.
- Structural analysis: single-crystal and powder diffractometric investigations.
- Scanning Electron Microscope.
- Chemical analysis: electron microprobe, X-ray fluorescence.
- Spectroscopic analyses: Mössbauer and vibrational.
Books
Texts
The topics treated in the course cannot be found in a unique book. Basic notions are contained in a few chapters of the following textbooks:
Tilley R., Crystals and Crystal Structures, 2006, Wiley.
Gualtieri A.F., Introduzione alle tecniche analitiche strumentali, 2019, libreriauniversitaria.it
Klein C., Mineralogia, 2004, Zanichelli, Bologna.
Bibliography
Putnis A., An Introduction to Mineral Sciences, 1992, Cambridge University Press
Lessons mode
Lessons in class room and practice in room.
The course will take place in the second semester: if the health emergency from COVID-19 will allow to carry out the lessons in presence, the course will be delivered in traditional mode, if vice versa it will not be possible, it will be delivered at a distance in accordance with what will be established by the competent authorities and the provisions of the University.
Frequency
Class attending is not mandatory, but strongly recommended.
Exam mode
Oral assessment (average time ca. 30 minutes).The final score reflects the analytical, verbal, quantitative and interpretative skills of the candidate, taking into account skills such as logical reasoning.To pass the exam the student must obtain a grade of not less than 18/30. The student must demonstrate that he/she has acquired a sufficient knowledge of mineral crystal-structure and experimental investigation strategies. To achieve a score of 30/30 cum laude, the student must instead demonstrate that he/she has acquired excellent knowledge of all the topics covered during the course, being able to link them in a logical and coherent way.
Example exam questions
What is a mineral?
What is polymorphism?
Arguments
- II semester
Sustainability goals
- Academic year2026/2027
- Degree program to which the course belongsExploration Geology
- Lesson code10620850
- Year and semester1st year - 2nd semester
- Activity typeAttività formative affini ed integrative
- Academic areaAttività formative affini o integrative
- SSDGEO/06
- Mandatory presenceNo
- LanguageITA
- CFU6 CFU
- Total duration60 hours
- Hours distribution24 classroom hours, 12 training hours, 24 laboratory hours