| 10626229 | ORGANIC SYNTHESIS [CHEM-05/A] [ITA] | 1st | 1st | 9 |
Educational objectives Organic Synthesis is an advanced branch of knowledge in the field of Organic Chemistry, that allows to build the molecular frame of complex targets not randomly but in a focused and efficient way. Organic Synthesis represents also an area of industrial expertise, as most of synthetic targets are bioactive molecules of high added value, and sustainability in their preparation process is an up-to-date challenge.
General educational objectives of the course are: to confer knowledge of the main strategies and methodologies in organic synthesis, and to improve knowledge in preparative organic chemistry processes’ set up by lectures and class practice. As expected results of the learning path, students will be able to project the synthesis of a simple organic compound by means of logic principles, to know how to realize a modern synthesis by the Green Chemistry approach and also to describe simple organic preparative procedures.
At the end of the course (specific objectives) students will be able to: have a wider knowledge of organic chemistry and especially organic synthesis, also by way of the rational approach to modern organic synthesis, i.e. the logic of organic synthesis (lectures); to devise synthetic routes to simple organic molecules as targets, and to have a basic knowledge in the field of green synthesis (lectures); to expand their knowledge in preparative organic chemistry (lectures and class practice). They will also be able, by applying cross knowledge in organic reactions, to evaluate the best synthetic path among many (examples in lectures and class practice) and to discuss synthetic plans with the correct scientific language (questions and examples in lectures and class practice). The in-depth knowledge of organic reactions topics will give students the ability to continue studying organic chemistry on their own.
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| 10626228 | [CHEM-04/A] [ITA] | 1st | 1st | 6 |
Educational objectives The course is dedicated to the knowledge deepening on the synthesis and behavior of polymeric materials in the solid state. The course is aimed at students who have already acquired basic information on chemistry and chemical-physics of macromolecules. In particular, through the specific study on the behavior of elastomeric, viscoelastic, crystalline and electronic conductor polymers, the student acquires skills on the correlations between the chemical structure of the materials and their properties. The course is organized in such a way as to give the student the opportunity to know the theories and models that describe the key characteristics of each type of material, the deviations from the models and the real behaviors. Moreover, through examples of experimental results on polymer materials properties, obtained by various techniques, the ability to choose the most appropriate type of instrumental analysis to characterize the material in relation to its application destination is stimulated. These skills are also developed through the solicitation of critical reading, besides textbooks, of scientific publications or technical reports on the properties of polymeric materials. With the knowledge acquired, the student will have skills on the principles and criteria of use of polymeric materials, may be able to predict the behavior of materials based on the analysis of the macromolecule structure and have the possibility to hypothesize or design the materials properties in relation to possible uses. Students will be able to easily enter both in the working world of the chemical industry of polymeric materials as well as in the scientific activity of the academic world and of research centers dealing with polymers. In addition, the information provided may be used to face with greater awareness the topics of other courses of concerning the study and application of polymers.
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| 10629805 | STRUCTURE OF MACROMOLECULES [CHEM-02/A] [ITA] | 1st | 1st | 6 |
Educational objectives The course aims to introduce the concepts of the structure of matter and the chemical-physical methods applied to structural characterization focusing on X-ray and Neutron diffraction techniques. Different X-ray diffraction techniques will be introduced such as wide angle X-ray diffraction (EDXD and ADXD) and the small angle x-ray scattering (SAXS) and their ability to characterize the structure over a wide spatial scale will be demonstrated (covering from interatomic distances to mesoscopic sizes).
Accurate knowledge of the theory of X-ray diffraction from an electron, an atom, a set of atoms and finally from a nanoparticle will be developed. The experimental data treatments will be explained with the aim of obtaining information on the structure of systems with different degrees of order: from disordered systems such as liquids, to crystalline and semicrystalline systems, to complex systems organized on the nanometric scale.
Furthermore, during the course the different theoretical models for the treatment of experimental data of macromolecular systems (polymers and biomolecules) will be introduced and related applications will be proposed and discussed.
Several laboratory experiments will be carried out demonstrating the ability of the X-ray diffraction technique for the structural study of disordered / complex systems. Diverse laboratory experiences will also be proposed to consolidate the theoretical knowledge and gain the practical ability to process experimental data. Through the laboratory experiences, the student will learn to collect diffraction data, will be able to process them, and, by the application of theoretical models, will extract the relevant structural parameters of the system under study.
At the end of the course, the student must have acquired skills regarding the general principles of X-ray scattering, the principles of the LAXS and SAXS experiment and the morphological properties of disordered / complex systems. The student will be able to select the most suitable experimental conditions for the study of the proposed systems, demonstrating the ability to apply the acquired skills. Furthermore, the student must know how to argue and defend the chosen options. He will have competence in extracting structural features of complex systems, such as polymer solutions, biomacromolecules solutions and complex fluids. At the end of the course the student must demonstrate the ability to frame the problem in the right context and to select the theoretical models best suited to its qualitative and quantitative resolution.
The final test will also evaluate the ability of analysis, synthesis and logical consistency in oral presentation and the ability of the student to communicate in an appropriate language at the level corresponding to Laurea Magistrale.
During the course the student will be proposed with scientific reports published in international journals together with the reference texts for further information that will be discussed in the classroom. This approach should favor the ability to learn and the habit of selecting various bibliographic sources, in Italian and in English. It should also stimulate the need for continuous updating, depending, for example, on the development of the Master's degree thesis or research doctorate. Furthermore students will be stimulated to propose selected systems, in order to apply the acquired techniques and correspondingly rationalise the relationship between microscopic features and macroscopic functionality.
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| 10627648 | SUSTAINABLE MATERIALS FOR INDUSTRY AND ENVIRONMENT [CHEM-04/A] [ITA] | 1st | 1st | 6 |
Educational objectives The educational objective of this course is to provide the student with adequate knowledge of the fundamental concepts of the chemistry of advanced materials applied to the environmental, agro-food, energy, biotechnological and cultural heritage sectors.
In fact, materials are at the heart of industrial innovation and represent indispensable factors for industrial competitiveness and sustainable development. One of the most important objectives is to develop advanced materials with new functions and better performance in use, for more competitive and safer products that allow the impact on the environment and the consumption of resources to be reduced to a minimum.
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| 10629705 | ANALYSIS AND CONTROL OF CHEMICAL PROCESSES [ICHI-01/C] [ITA] | 1st | 2nd | 9 |
Educational objectives MODULE I
A – Knowledge and Understanding
Students who have passed the exam will be able to know and understand (acquired knowledge):
• Basic knowledge of statistical inference for data analysis (confidence intervals, hypothesis testing, and analysis of variance);
• Basic knowledge of experimental design and related statistical analysis (factorial experiments and randomized block experiments for comparing two samples);
• Basic knowledge of linear (univariate and multivariate) and nonlinear regression analysis.
B – Applied Skills
Students who have passed the exam will be able to:
• Apply techniques for experiment planning and related statistical data analysis;
• Perform linear and nonlinear regression of experimental data and the corresponding statistical analysis;
• Use data analysis and regression tools available in commonly used software (e.g., Excel), as well as in specialized technical software for experiment design and data analysis (e.g., JMP).
C – Independent Judgment
• Be able to formulate their own assessment and/or judgment based on the objective interpretation of available experimental data in relation to the comparison of samples with reference values, two samples, or multiple samples;
• Be able to identify optimized procedures to improve system understanding by identifying sources of data variation through completely randomized or block experiments;
• Have the practical ability to take initiatives and make decisions regarding the choice of the best empirical model to represent the experimental data obtained, based both on upstream statistical analysis and the evaluation of different possible models through statistical discrimination.
D – Communication Skills
• Be able to explain to non-experts the basic concepts of statistical data analysis, experimental design, and data regression with linear and nonlinear models;
• Describe methodologies for data analysis, experimental design, and parameter regression of linear and nonlinear models using technically accurate language.
E – Learning Ability
• Possess the learning skills necessary for continuous improvement in the fields of data analysis, experimental design, and model parameter regression;
• Be able to draw from various bibliographic sources, both in Italian and in English, to acquire new competencies.
MODULE II
A – Knowledge and Understanding
Students who have passed the exam will be able to know and understand (acquired knowledge):
• The issues related to the control of chemical processes, and how these issues can be addressed through the formulation and systematic application of mathematical models;
• The basic concepts necessary for system dynamics analysis;
• The main strategies used for chemical process control;
• The basic concepts necessary for designing the control system of a chemical process.
B – Applied Skills
Students who have passed the exam will be able to:
• Develop lumped-parameter mathematical models of chemical processes through the application of conservation principles;
• Evaluate, through the analysis of the formulated mathematical models, how a process system's dynamics change with variations in operating and design parameters;
• Analyze the dynamics of a nonlinear system through the study of its linearization;
• Determine the response of a linear system to changes in input variables;
• Determine the parameters of basic control systems for chemical processes.
C – Independent Judgment
• Be able to formulate their own assessment and/or judgment based on the interpretation of available information in the context of chemical process analysis and control;
• Be able to identify and gather additional information to achieve greater awareness;
• Have the practical ability to take initiatives and make decisions, taking into account various relevant aspects of chemical process analysis and control.
D – Communication Skills
• Be able to explain to non-experts the basic concepts of system dynamics and how the development and application of mathematical models allow the resolution of design and control issues in chemical processes;
• Describe methodologies for chemical process control using technically accurate language.
E – Learning Ability
• Possess the learning skills necessary for continuous improvement in the study of the dynamics and control of chemical processes;
• Be able to draw from various bibliographic sources, both in Italian and in English, to acquire new competencies.
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| 10629251 | [CHEM-04/A] [ITA] | 1st | 2nd | 6 |
Educational objectives The student will be guided to understand the molecules, polymers and the most important materials used in the biomedical field. It will have to know how to relate the main chemico-physical and structural properties of the biomaterials with the functions carried out in the organism in relation to the mechanisms of interaction with the organism itself. He will learn the most important properties and uses of metals, ceramics and biopolymers, in particular polypepetides and polysaccharides, of biomedical interest.
For a specific biomedical task, it will have to be able to identify the most suitable combination of biomaterials to solve the problem.
The student will develop critical and judgmental skills through the discussion in the classroom of the topics covered during the lectures.
These objectives will be achieved by means of frontal lessons, watching scientific videos and reading advanced bibliographic material (reviews, examples of patents, etc.).
They could apply their knowledge and understanding, and problem solving abilities in new or unfamiliar environments within broader (or multidisciplinary) contexts related to biomaterials.
At the end of the course, with the knowledge acquired, the student, together with other professionals such as doctors, biologists and engineers, will be able to propose and develop ideas for the design of a new biomedical device.
The ability to communicate what has been learned clearly, fully and rationally motivating what is reported, will be evaluated through an oral exam.
At the end of the course the student will have acquired the ability to continue the study in a highly autonomous way on any topic, even advanced, which concern biomaterials and biopolymers
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| 10627670 | [CHEM-04/A] [ITA] | 1st | 2nd | 9 |
Educational objectives The course is organized in such a way as to provide the master's degree students with in-depth information on some experimental techniques used for the characterization of polymeric materials. Through the analysis of the acquired results the correlations between the observed properties and the structure of the materials and their fields of application will be highlighted.
In particular, the course describes topics relating to surface tension of polymer solids, dynamo-mechanical analysis, kinetics of crystallization, applications of Fourier transform infrared spectroscopy in the characterization of polymers and the electrical properties of insulating and conducting polymers. For each topic covered, the course is developed in three phases.
In the first one, the physical and chemical quantities measured by the instrumental technique, the theories that describe the analyzed phenomena, the correlations between the chemical structure of the materials and their behaviour will be analysed in detail.
In the second phase, the instrumentation and the experimental procedures to be used in relation to the information to be acquired will be described. The used procedures will be compared with those proposed, if existing, by international regulations.
In the third phase, the experimental tests will be carried out and data will be acquired for the subsequent elaborations. The results obtained will be analyzed according to the theories described in the first phase.
The student will be able to manage the used instrumentation. Moreover, he will acquire the appropriate awareness to analyze which experimental and instrumental parameters are important to carry out characterization tests, also by employing techniques not used in the course. The importance dedicated to the analysis and processing of experimental data is aimed at acquiring the ability to critically apply mathematical models able to describe and, therefore, predict the behavior of materials, even in conditions not directly examined. The achievement of this objective is obtained through group work, drafting of written technical reports, the presentation of the results achieved and numerical exercises on macromolecular problems.
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| [N/D] [ITA] | 1st | 2nd | 6 |
| 10626242 | [CHEM-04/A] [ITA] | 2nd | 1st | 9 |
Educational objectives The main aim is to provide knowledge on the fundamental principles of heterogeneous catalysis and of the gas-solid reactivity. The course will be useful to acquire an integrated methodology to correlate structural and reactivity features of solid materials and gaseous reactants with kinetic and thermodynamics features of the reactions.
Students are expected to:
1. learn, by following a multidisciplinary approach, the fundamental methods for the catalysts preparation and characterization (in the bulk and at the surface), the mechanisms of surface reactions (adsorption of reactants, surface reactions, desorption of products) and some applications of catalysts in industrial processes and for the solution of environmental problems.
2. use of a multidisciplinary approach by analysing examples from research or industry field. The student will apply the basic principles, previously acquired in the main courses of General, Inorganic and Physical Chemistry, to understand catalytic phenomena and will be able to evaluate in a qualitative and quantitative way:
- the main kinetic parameters for describing catalysts activity and selectivity, paying attention to the diffusion aspects;
- the main morphological and physico-chemical properties (composition, structure, dispersion) of the catalysts determining the catalytic performance.
3. move the first steps in the interpretation of experimental results reported in the scientific literature.
4. be able to present in a synthetic and appropriate way the acquired knowledge.
5. be able to argument his choices, thus facing further studies with a certain degree of autonomy.
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| 10628805 | APPLIED SPECTROSCOPIC METHODS [CHEM-02/A] [ITA] | 2nd | 1st | 6 |
Educational objectives This course offers an introduction to the Spectroscopic Methods used for the study of chemical and macromolecular systems. The different spectroscopic techniques such as rotational, vibrational and electronic spectroscopy and nuclear magnetic resonance will be described starting from the quantum mechanical principles of the reference models. The most significant applications for the characterization of chemical and macromolecular systems will then be considered.
The aim of the course is to provide the student with a theoretical and practical knowledge of the physical basis of the most widely used spectroscopic techniques and their range of applications to the study of chemical and macromolecular systems
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| 10629199 | [CHEM-02/A] [ITA] | 2nd | 1st | 6 |
Educational objectives In accordance to the first two Dublin descriptors, at the end of the course the student will have understood the following concepts:
a) meaning of conducting polymer and doping phenomena in semiconducting polymers;
b) principles of synthesis and characterization of conducting polymers;
c) materials science at the basis of the choice of specific polymers as active materials of devices for electrochemistry, optics, electronics and sensors
The student will use the concepts grasped during the course of Physical Chemistry of the Solid State and Nanostructured Materials to prepare and characterize polymeric materials with different properties of electrical conduction. The course has also the finality of developing the communication skills of the student (fourth Dublin descriptor). This is realized through questions during classes and in the final exam.
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| [N/D] [ITA] | 2nd | 2nd | 6 |
| AAF1162 | [N/D] [ENG] | 2nd | 2nd | 4 |
| AAF1147 | OTHER USEFUL SKILLS FOR INCLUSION IN THE WORLD OF WORK [N/D] [ITA] | 2nd | 2nd | 1 |
| AAF1029 | Final exam [N/D] [ITA] | 2nd | 2nd | 31 |
Educational objectives The final examination for the attainment of the Master’s Degree in Industrial Chemistry consists of carrying out an original research activity undertaken by the student under the supervision of a supervisor. This work concludes with the submission of a written thesis and its presentation and discussion during a public session before an appointed committee, which will issue the final evaluation. The number of ECTS credits allocated to this activity is specified in the Degree Programme Regulation.
The final examination is a crucial moment in which the student demonstrates the ability to develop an original and applied research project consistent with the educational objectives of the chosen curriculum. The student must also demonstrate methodological competence, analytical and synthesis skills, scientific communication abilities, and the capacity to apply advanced theoretical and experimental knowledge to complex problems in the industrial chemistry sector.
The research phase includes data collection, which may be carried out through experiments, simulations, or theoretical and bibliographic analyses. The results obtained must be examined with methodological rigor, compared with the relevant scientific literature, and interpreted to highlight the original aspects and innovative contribution of the work. It is essential that the student shows the ability to address and resolve critical issues that arise during the research process.
Writing the thesis is an essential component of the final examination. The document must include: an introduction outlining the context of the work and the objectives of the project; a critical review of the literature describing the state of the art and identifying the knowledge gaps the project aims to address, thereby defining the research goals; a section on materials and methods documenting the techniques and tools employed; a presentation of the results supported by graphs, tables, or diagrams, followed by a discussion interpreting their significance and emphasizing the original contribution; conclusions summarizing the main findings and illustrating possible future developments; and an accurate bibliography including all consulted sources.
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