THREE-DIMENSIONAL MODELING

Course objectives

The course provides students with knowledge of archaeometallurgical techniques, smelting principles, phase diagrams of metal alloys, and thermal analyses (TGA, DSC). It covers crystalline structure analysis using X-ray diffraction (XRD) and the interpretation of XRD patterns. Students will develop skills to evaluate phase compositions, differentiate between glass and crystals, and solve problems related to TGA, DSC, and XRD. They will also gain autonomy in applying these techniques, communicate in English, and improve their learning and reflection abilities. The course enhances students’ understanding of materials science within the context of cultural heritage conservation, with a particular focus on metals, alloys, and ceramics. It equips students with the skills to develop protocols for the characterization of inorganic materials using phase diagrams, thermal analysis (TGA and DSC), and X-ray diffraction (XRD). Students will study atomic arrangements in inorganic materials, influenced by metal types, alloy compositions, and metallurgical processes. Thermal analysis techniques will be presented as essential tools for assessing the behavior and stability of materials under heat treatment. XRD will be introduced as a key method for investigating crystalline structure. By integrating these analytical techniques with theoretical knowledge, students will be able to design effective and targeted characterization protocols. A - Knowledge and understanding OF 1) archaeometallurgical techniques and the principle of smelting OF 2) phase diagrams of various metal alloys OF 3) thermal analyses of materials: thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) OF 4) crystalline structures with different atomic packing arrangements OF 5) X-ray diffraction (XRD) techniques OF 6) interpretation of XRD patterns and determination of crystalline structures … B - Application skills OF 7) evaluate phase types, phase numbers, their composition ratios, and the composition within a single phase using phase diagram OF 8) explain the differences between glass and crystals OF 9) solve problems of TGA, DSC, and XRD analyses … C - Autonomy of judgment OF 10) comprehend patterns obtained from TGA, DSC, and XRD analyses OF 11) define phase structures using these techniques in combination with a phase diagram OF 12) construct evaluation procedures for inorganic materials D - Communication skills OF 13) working command of English OF 14) draw simple charts and write sentences E - Ability to learn OF 15) evaluating and analyzing your own understanding OF 16) asking questions if something unclear OF 17) developing own study program independently OF 18) having basic computer skills

Channel 1
AKIKO TSURUMAKI Lecturers' profile

Program - Frequency - Exams

Course program
1) Learn about the archaeometallurgy techniques; 2) Understanding phase diagrams of different metal alloys; 3) Learn thermal analyses of inorganic materials: thermal gravimetric analysis (TGA) and differential scanning calorimetry (DSC); 4) Describe the differences between crystal and glass; characterize the different modes of atomic packing; remember the principles of X-ray diffraction techniques; 5) Develop a protocol to evaluate conservation and restoration procedure for new cultural heritage materials.
Prerequisites
a) Knowledge of English; b) High school level knowledge of History and Art History; c) University level knowledge of General Chemistry: atomic structure, chemical bonds, electronegativity, intermolecular forces, saturated and unsaturated organic compounds, functional groups, phase transition, equilibrium in solution: acid-base and pH, complexation, oxidation-reduction reactions, and redox potential.
Books
i) Lecture notes prepared by the teacher ii) Introduction to Materials Science, Authors: Jean P Mercier, Gerald Zambelli, Wilfried Kurz, Elsevier Science & Technology
Teaching mode
Lectures (16 hours), Exercises (12 hours)
Exam mode
In order to pass the exam, it is necessary to obtain a grade not lower than 18/30. The student must demonstrate that he/she has acquired a sufficient knowledge of the material properties of artworks, the origin of their degradation, and the strategies used for their conservation and restoration. In order to obtain a score of 30/30 cum laude, the student must demonstrate to have acquired an excellent knowledge of all the topics covered during the course, being able to connect them in a logical and coherent way. Some formative evaluation questionnaires will be proposed during the course.
Lesson mode
Lectures (16 hours), Exercises (12 hours)
  • Academic year2025/2026
  • CourseScience and Technology for the Conservation of Cultural Heritage
  • CurriculumScience and Technology for the Conservation of Cultural Heritage - in lingua inglese
  • Year1st year
  • Semester2nd semester
  • SSDCHIM/12
  • CFU3